課程大綱

課程資訊

課程名稱

分析化學乙下
ANALYTICAL CHEMISTRY (B)(2)

開課學期

98-2

授課對象

生化科技學系

授課教師

張哲政

課號

Chem2012

課程識別碼

203 211B2

班次

學分

全/半年

全年

必/選修

必帶

上課時間

星期五3,4(10:20~12:10)

上課地點

普406

備註

請依指定修習院系班次修習。詳化學系選課須知。先修：普化。上下學期需選同一班次。
總人數上限：80人

Ceiba 課程網頁

http://ceiba.ntu.edu.tw/982analychem_b2_02

課程簡介影片

核心能力關聯

本課程尚未建立核心能力關連

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課程概述

This course extends the knowledge of the analytical chemistry to include the fundamental principles and application of modern instrumental methods including spectroscopic, spectrometric, and separation methods. The topics covered have applications to many subject areas in Natural Sciences, Life Science and Engineering.
This course is presented in a lecture/discussion format. The content of the course includes:
Introduction to Instrumental Analysis
Problem Solving
Method Choice
Classification
Electrical Domains
Calibration
Fundamentals of Spectroscopy/Spectrometry
Electromagnetic Radiation
Property of Light
Absorption and Emission
Absorbance and Transmission
Beer’s Law
Spectrometer
General Design
Source
Monochromator
Detector
Optical Sensor
UV and Visible Absorption Spectrometry
Radiation Spectroscopic Process
Solvent Effect
Effect of Multichromophore
Detector
Spectral Analysis
Standard Addition Method
Luminescence Spectrometry
Photoluminescence
Quantum Yield
Fluorescence Systems
Fluorometric Reagents
Synchronous Spectrum
Infrared Absorption Spectrometry
Dipole Moment
Vibrational Mode
Fourier Transform
Interferometer
Detector
Spectral Analysis
Raman Spectroscopy
Immunoassay
Enzyme-Linked ImmunoSorbent Assay (ELISA)
Lab-on-a-Chip
Surface Plasmon Resonance (SPR)
Attenuated Total Reflectance
Surface Plasmon
Evanescent wave
Atomic Spectrometry
Atomization
Temperature Effect
Interference
Mass Spectrometry
Ion Source
Mass Spectrometer
Mass Spectrum
Inductively Coupled Plasma-Mass Spectroscopy
Nuclear Magnetic Resonance Spectroscopy
Nuclear Magnetic Resonance
Relaxation Mode
Chemical Shift
Environmental Effect
Analytical Separation
Solvent Extraction
Chromatography
Efficiency of Separation
Bands Spread
Gas Chromatography
Separation Process
Injection and Detection
Detector
Sample Preparation
High-Performance Liquid Chromatography
Chromatographic Process
Injection and Detection
Reversed-Phase Separation
Gradient Separation
Ion-Exchange Chromatography
Molecular Exclusion Chromatography
Capillary Electrophoresis

課程目標

This course provides students with the background theory and operation principles of instrumental analysis methods. The specific objectives of the course are as follows:
- to become familiar with the various spectroscopies, spectrometries, and separation methods currently available
- to develop an understanding of the theories upon which the principles of common spectroscopic, spectrometric, and separation procedures are based
- to understand the correlations of spectroscopic/spectrometric/separation analysis concepts and of various controllable and measurable quantities
- to learn how the different instrumental methods are used to analyze samples
- to understand the limitations and strengths of different analysis approaches
- to gain skill and competence in the use of related analytical standards/references
- to learn to apply chemical equilibria and stoichiometry to solve spectroscopic/spectrometric/separation analysis problems

課程要求

Make-up exams will not be permitted to those who miss the midterms or the final. Students should present records of clinic visits for missing the exam due to illness.
Good, participatory attendance is essential to successful mastery of course material. Although the attendance will not be monitored daily, it is suggested that you do not take this course if you cannot come to the class.

預期每週課後學習時數

Office Hours

每週五 12:10~13:10 備註： It starts right after the class and ends whenever the last student finishing asking his/her questions.

指定閱讀

Holler, Skoog, and Crouch, Principles of Instrumental Analysis, 6th Ed.,
Thomson Brooks/Cole, ISBN: 0-495-01201-7

參考書目

James W. Robinson, Undergraduate Instrumental Analysis, Marcel Dekker
Francis Rouessac, Annick Rouessac, Chemical Analysis-Modern Instrumentation Methods and Techniques, Wiley,
K. A. Rubinson, J. F. Rubinson, Contemporary Instrumental Analysis, Prentice-Hall, Inc.
Daniel C. Harris, Quantitative Chemical Analysis, W.H. Freeman and Company
Skoog, West, Holler, Crouch, Fundamentals of Analytical Chemistry, Thomson

評量方式
(僅供參考)

No.	項目	百分比	說明
1.	First Exam	30%	The exams are primarily problems and short essays, not true-false or multiple choice. They will emphasize the course objectives of understanding the background theory, operation principles, design, applications, strengths, and limitations of the chemical analysis methods introduced. The content of the tests includes the materials discussed in your textbook as well as those taught in the class. Calculators used in the exam cannot contain any dictionary function.
2.	Second Exam	30%	The exams are primarily problems and short essays, not true-false or multiple choice. They will emphasize the course objectives of understanding the background theory, operation principles, design, applications, strengths, and limitations of the chemical analysis methods introduced. The content of the tests includes the materials discussed in your textbook as well as those taught in the class. Calculators used in the exam cannot contain any dictionary function.
3.	Final Exam	40%	The exams are primarily problems and short essays, not true-false or multiple choice. They will emphasize the course objectives of understanding the background theory, operation principles, design, applications, strengths, and limitations of the chemical analysis methods introduced. The content of the tests includes the materials discussed in your textbook as well as those taught in the class. The final test is a comprehensive exam and will require you to integrate the class material in a meaningful way. Calculators used in the exam cannot contain any dictionary function.

課程進度

週次

日期

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